Nitric Acid, ASTM A, Practice C, (Huey Test) The specimens are boiled for five periods, each of 48 hours, in a 65 per cent solution of nitric acid. The corrosion. employed to measure the relative susceptibility of austenitic stainless steels to intergranular attack. ASTM A Practice C, boiling nitric acid test is also known . Ferric Sulfate – Sulfuric Acid, ASTM A – Practice B (Stretcher Test). Ferric Sulfate Nitric Acid, ASTM A, Practice C, (Huey Test). Nitric Acid, ASTM A
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The test evaluates asstm resistance of extra-low-carbon steels to sensitization and intergranular attack from welding or heat treatment processes.
Our knowledgeable scientists have the experience and expertise necessary to determine the most appropriate intergranular attack testing methods for your material while providing actionable results you can rely on.
This test is used exclusively to determine corrosion in areas high in chromium carbide formations, and is not as effective for intergranular attack caused by other means. Please specify the maximum allowable corrosion rate and any available data on the sensitizing heat treatment performed.
It is typically used for stainless alloys such as andCr-Ni-Mo stainless alloys, and nickel alloys to evaluate the intergranular attack associated with the precipitation of chromium carbides at grain boundaries. ASTM A is a common intergranular corrosion testing method that can quickly screen batches of material to determine corrosion susceptibility. These tests are often run as a qualification test to ensure each batch of stainless steel is properly prepared.
For example, many low-carbon and stabilized stainless steels e. However, when a material is exposed to high temperatures for long periods of time, a process called sensitization may occur.
Choosing the correct method s rely on a complete understanding of your material and processes, as well as the concept of corrosion itself. Classification of the structure after A Practice A analysis will determine if the material is acceptable or if additional q262 is required.
ASTM A Intergranular Corrosion Testing and Analysis
The Copper Sulfate Test is especially effective for determining susceptibility to intergranular attack for low carbon steels. Methods for preparing the test specimens, rapid screening tests, apparatus setup and testing procedures, and asm and report contents are described for each testing practice. This practice includes boiling the sample for 24 to hours in the solution above, and measures the materials performance quantitatively. Discover perspectives, resources, and advice from our world-leading Engaged Experts.
This specification covers the standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels.
Asttm first and fastest step is the ASTM A Practice A, a rapid same-day screening method in Oxalic acid to determine the susceptibility to intergranular corrosion. The etch structure types used to classify the specimens are: ASTM A testing is a popular method of choice due to the variety of practices available and the relatively short turnaround for results. The Huey test works well to analyze chromium depleted regions and intermetallic precipitates, such as sigma phase, and is also used for materials in strongly oxidizing environments such as nitric acid.
Practice F, is a hour weight-loss based analysis that provides a quantitative measure of the materials performance, and is commonly used to analyze as-received stainless steels.
The bent samples are examined at low magnification, where the appearance of cracks or fissures indicate intergranular attack. Share on Tumblr Print. Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed pactice and does not show signs of corrosion susceptibility. The Strauss test is commonly used to evaluate the heat-treatment of as-received material, the effectiveness of alloying additions of elements such as Nb and Ti, or the effectiveness of reducing carbon content to resist intergranular attack.
This simple etching technique is used as a quick screening method to ensure that a material is free of intergranular corrosion susceptibility. The oxalic acid test is commonly used before the Strauss test to determine if a sample is susceptible; samples that pass method 2a62 will generally show low corrosion rates in the Strauss test.
This abstract is a brief summary of the referenced standard.
It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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For example, in highly oxidizing solutions, intergranular attack practife occur due to intermetallic phases, while attack of carbides may occur somewhat less oxidizing solutions. ASTM does not give any warranty express or implied or make any representation that the contents of this abstract are accurate, complete or up to date.
G2MT Labs is one of the few labs to offer all five ASTM A corrosion testing practices, as well as the expertise to help you determine which tests to use, what to do if a test fails, and other corrosion consulting as needed. Strauss test specimens are boiled in a Copper Sulfate – Sulfuric Acid mixture for 15 hours.
Please refer to the specification for more details. In SEM analysis, intergranular corrosion is clear by the dark lines where the grain boundaries are eaten away.
Metals like stainless steels and aluminum contain elements such as niobium and chromium, often integrated because of their natural corrosion resistance. Learn more about our laboratories – where they are located; the unique capabilities they have and how they can help you solve your technical and commercial challenges. It depends on which Practice is selected, but typically ranges from to days for different tests.
Historical Version s – view previous versions of standard. Practice A, the oxalic acid etch test is used as a rapid technique to screen samples of certain stainless steel grades to ensure they are not susceptible to intergranular attack sensitization.